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- W2996543758 abstract "Abstract The regioselective anti ‐carboindation of ynamides by using InBr 3 and silylated nucleophiles was developed to synthesize ( Z )‐β‐(carbonylamino)alkenylindiums. The X‐ray crystallographic analysis of an alkenylindium suggested that the reaction proceeded in an anti ‐addition fashion. In contrast to reported syn ‐carbometalations of ynamides by using organometallics, a cooperation of InBr 3 and silylated nucleophiles to ynamides achieved an anti ‐addition, which was supported by DFT calculations. The scope of substrates included various ynamides and silylated nucleophiles, such as silyl ketene acetals and silyl ketene imines. The transformation of synthesized alkenylindiums by iodination, radical coupling, and Pd‐catalyzed cross‐coupling successfully afforded trisubstituted enamines with high regio‐ and stereoselectivities." @default.
- W2996543758 created "2019-12-26" @default.
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- W2996543758 date "2020-02-21" @default.
- W2996543758 modified "2023-10-01" @default.
- W2996543758 title "Synthesis of ( <i>Z</i> )‐β‐(Carbonylamino)alkenylindium through Regioselective <i>anti</i> ‐Carboindation of Ynamides and Its Transformation to Multisubstituted Enamides" @default.
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- W2996543758 doi "https://doi.org/10.1002/chem.201905175" @default.
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