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- W2996953095 abstract "An efficient palladium-catalyzed approach to access various functionalized (Z)-3-benzylidene-isoindoline-1-ones and (Z)-3-benzylidene(imino)isobenzofuranones via a denitrogenative tandem alkynylation/cyclization reaction of 1,2,3-benzotriazin-4(3H)-ones with aromatic terminal alkynes is described. Furthermore, a denitrogenative ortho-alkynylation reaction of 1,2,3-benzotriazinones with aliphatic terminal alkynes is also developed. The reaction proceeds through a five-membered azapalladacyclic intermediate with the extrusion of a nitrogen molecule. The significance of the reaction is also demonstrated by a one-pot synthesis of (Z)-3-benzylideneisobenzofuran-1(3H)-one derivatives in good to high yields." @default.
- W2996953095 created "2020-01-10" @default.
- W2996953095 creator A5040027260 @default.
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- W2996953095 date "2019-12-30" @default.
- W2996953095 modified "2023-10-07" @default.
- W2996953095 title "Palladium/Copper-Catalyzed Denitrogenative Alkylidenation and <i>ortho</i>-Alkynylation Reaction of 1,2,3-Benzotriazin-4(3<i>H</i>)-ones" @default.
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- W2996953095 doi "https://doi.org/10.1021/acs.orglett.9b04297" @default.
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