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- W29990533 abstract "For determination of small amounts of U(6+) in UO/sub 2/ use is made of potentiometric titration with a solution of Ti/sub 2/(SO/sub 4/)/sub 3/. To 4 to 5 g UC/sub 2/ in a Pt-dish are added 10 ml concentrated HF, 30 ml water, and the mixture is heated until a green precipitate (UF/sub 4/) is formed containing no black particles. Thereafter the contents of the dish are diluted with water to 100 ml, 10 ml of the resulting solution are transferred to the potentiometric titration cell (with Pt- and Hg/sub 2/Cl/sub 2/-electrodes), 10 ml water and 3 g Rochelle salt are added and the temperature is raised to 70 deg . The titration is carried out with approximately 0.05 N solution of Ti/sub 2/(SO/sub 4/)/sub 4/N H/sub 2/SO/sub 4/. CO/sub 2/ is added to remove O/sub 2/ and to stir the solution. The results so obtained show good reproducibility but are characterized by a positive error. Use of H/sub 2/SO/sub 4/ for dissoiving the sampie results in analysis dnta which are much too high, but addition of the acid to the prepared solutions does not affect accuracy of the results." @default.
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- W29990533 date "1958-01-01" @default.
- W29990533 modified "2023-09-27" @default.
- W29990533 title "POTENTIOMETRIC DETERMINATION OF SMALL AMOUNTS OF HEXAVALENT URANIUM IN URANIUM DIOXIDE" @default.
- W29990533 hasPublicationYear "1958" @default.
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