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• W2999402956 abstract "A transition-metal-free deoxygenative C–H amination reaction of azine-N-oxides with acyl azides is described. The initial formation of an isocyanate from the starting acyl azide via a Curtius rearrangement can trigger a [3 + 2] dipolar cycloaddition of polar N-oxide fragments to generate the aminated azine derivative. The applicability of this method is highlighted by the late-stage and sequential amination reactions of complex bioactive compounds, including quinidine and fasudil. Moreover, the direct transformation of aminated azines into various bioactive N-heterocycles illustrates the significance of this newly developed protocol." @default.
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• W2999402956 date "2020-01-06" @default.
• W2999402956 modified "2023-10-16" @default.
• W2999402956 title "Deoxygenative Amination of Azine-<i>N</i>-oxides with Acyl Azides via [3 + 2] Cycloaddition" @default.
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• W2999402956 doi "https://doi.org/10.1021/acs.joc.9b03173" @default.
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