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- W3000254976 abstract "The inside cover picture, designed by Lakshman and co-workers, illustrates a diverse set of hydrogenations that can be conducted without use of external hydrogen gas (compressed gas). 4-Methylmorpholine (NMM), tetrahydroxydiboron [B2(OH)4], and 5% Pd on charcoal work in concert to cause reductions of aryl halides and triflates, alkenes, alkynes, aldehydes, and azides, as well as cleavage of benzylic ethers and N-Cbz groups. Based on the mechanistic knowledge gained in the study, aromatic deuteriations have also been accomplished using N,N-bis(methyl-d3)pyridin-4-amine (DMAP-d6) and B2(OD)4. H2 gas appears to be formed in these reactions and this has been observed by 1H NMR and GC analysis. Details of this work can in found in the full paper on pages 166–176 (K. A. Korvinson, H. K. Akula, C. T. Malinchak, D. Sebastian, W. Wei, T. A. Khandaker, M. R. Andrzejewska, B. Zajc, M. K. Lakshman, Adv. Synth. Catal. 2020, 362, 166–176; DOI: 10.1002/adsc.201901099)." @default.
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- W3000254976 date "2019-12-30" @default.
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- W3000254976 title "Cover Picture: Catalytic Reductions Without External Hydrogen Gas: Broad Scope Hydrogenations with Tetrahydroxydiboron and a Tertiary Amine (Adv. Synth. Catal. 1/2020)" @default.
- W3000254976 doi "https://doi.org/10.1002/adsc.201901549" @default.
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