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- W3000431005 abstract "An energy-efficient and environment-friendly approach to prepare porous monodispersed micro-sized silica particles with methyltrimethoxysilane (MTMS) as the precursor is described. The particles were synthesized by a two-step hydrolysis/condensation procedure, with post-synthetic aging and calcination for methyl group removal. They show uniform spherical morphology, narrow particle size distribution (D90/10, 1.2–1.6), tailored particle size (3, 5, 7 μm) and mesopore structure (10, 13 nm), which can be directly used as packing materials for HPLC without size classification. C18, sulfonate, and C18/sulfonate mixed-mode stationary phases were produced by a green vapor deposition method based on the synthesized silica particles. The newly synthesized C18 phase exhibits mechanical stability, kinetic behavior and separation performance expected from the commercial C18 column. The C18/sulfonate phase exhibits prominent mixed-mode retention behavior which can be applied to the simultaneous separation of multiple substances in the compound drugs." @default.
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- W3000431005 date "2020-05-01" @default.
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- W3000431005 title "Energy-efficient and environment-friendly method to prepare monodispersed silica stationary phases for simultaneous separation of compound drugs" @default.
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- W3000431005 doi "https://doi.org/10.1016/j.chroma.2020.460866" @default.
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