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- W3000487848 abstract "Abstract The performance of a leaded bronze alloy with CuSn 7 Pb 15 (wt %) chemical composition is studied as a cathode material for CO 2 electroreduction (CO 2 RR) in aqueous 0.5 M KHCO 3 electrolyte. It was found that the catalytic characteristics of the proposed CO 2 RR electrocatalyst are dominated by elemental lead. Surface characterization by means of digital 3D optical microscopy, white light interferometry, scanning electron microscopy (SEM), energy dispersive X‐ray spectroscopy (EDX) and scanning auger microscopy (SAM) revealed that segregated Pb clusters embedded in a Cu‐rich Cu/Sn matrix are, to a large extent, dispersed on the cathode surface upon sample preparation through mechanical polishing. Identical location SEM‐EDX studies before and after CO 2 electrolysis revealed that further Pb surface redistribution takes place under operando CO 2 RR conditions, provided sufficiently high potentials are applied. The as‐prepared electrocatalyst proved to be a suitable and powerful alternative for the selective and efficient production of formate (maximum achieved faradaic efficiency and partial current density for formate are 58.6 % and −11.08 mA cm −2 at −1.07 V and −1.17 V vs. RHE, respectively). Moreover, in comparison to neat lead, this material can be handled with less precaution." @default.
- W3000487848 created "2020-01-23" @default.
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- W3000487848 date "2019-04-15" @default.
- W3000487848 modified "2023-09-30" @default.
- W3000487848 title "Leaded Bronze Alloy as a Catalyst for the Electroreduction of CO <sub>2</sub>" @default.
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- W3000487848 doi "https://doi.org/10.1002/celc.201900537" @default.
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