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• W3000688981 abstract "We report novel materials for calcium phosphate mineralization processes. These materials were synthesized via a three-step procedure starting from chitosan. In a first step, N-guanidinium-chitosan acetate was prepared via a direct guanylation reaction with cyanamide. This intermediate was then used as a cationic polymer substrate for attracting two functional anionic silica precursors, which subsequently allowed accessing new ionic hybrid materials via sol-gel chemistry. These N-guanidinium-chitosan acetate/silica hybrid materials, containing either sulfonate or carboxylate groups, were characterized using solid state 13C NMR, 29Si NMR and FT-IR spectroscopy. Finally, these two ionic hybrids were used as templates for in-vitro biomimetic calcium phosphate mineralization using simulated body fluid solution. We could show that the two ionic hybrids act as versatile templates for biomineralization, inducing the formation of hydroxyapatite, as proved from XRD, SEM, EDX, TEM and TGA. The current results suggest that the new ionic hybrids may be promising candidates for bone tissue engineering applications." @default.
• W3000688981 created "2020-01-23" @default.
• W3000688981 creator A5003791938 @default.
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• W3000688981 date "2020-03-01" @default.
• W3000688981 modified "2023-10-17" @default.
• W3000688981 title "Synthesis and characterization of N-guanidinium chitosan/silica ionic hybrids as templates for calcium phosphate mineralization" @default.
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• W3000688981 doi "https://doi.org/10.1016/j.ijbiomac.2020.01.046" @default.
• W3000688981 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/31917982" @default.
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