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- W3001567989 abstract "Most of the vitrimers based on ester linkages reported so far contain a Lewis acid or a strong organic base as the transesterification catalyst. The recyclability and reusability of these vitrimers are dependent on the catalyst retention, stability, and sintering issues. Herewith, a set of β-activated ester-based vitrimers are reported that can be thermally reprocessed at ∼150 °C under catalyst-free conditions. The relaxation temperature decreases to 110 °C in the presence of Sn(Oct)2. Importantly, the precursor of these vitrimers, malonic ester, is a cost-effective naturally occurring ester and can be extracted from various fruit juices. As a proof of concept, poly(hydroxyethyl methacrylate) is used as the hydroxyl precursor for the synthesis of vitrimers. These vitrimers display an adequate tensile strength (11.3–33.0 MPa), elongation (80–290%), and resilience. The materials can be effectively self-healed and reprocessed in the presence of heat without sacrificing the tensile properties. The vitrimers b..." @default.
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- W3001567989 date "2020-01-22" @default.
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- W3001567989 title "Catalyst-Free Partially Bio-Based Polyester Vitrimers" @default.
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- W3001567989 doi "https://doi.org/10.1021/acsapm.0c00016" @default.
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