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- W3003335752 abstract "Abstract A visible‐light‐promoted photochemical protocol is reported for the coupling of aryldiazoacetates with boronic acids. This photochemical reaction shows great enhancement compared to the same protocol performed in the absence of light. Except for a few cases, the room temperature coupling in the dark (thermal process) generally does not work. When it does, it is likely to also involve free carbenes as key intermediates. Alternatively, photochemical reactions show a broad scope, can be performed under air and tolerate a wide variety of functional groups. Reaction‐evolution monitoring, DFT calculations and control experiments have been used to evaluate the main aspects of this intricate mechanistic scenario. Biologically active molecules Adiphenine, Benactyzine and Aprophen have been prepared as examples of synthetic applications." @default.
- W3003335752 created "2020-02-07" @default.
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- W3003335752 date "2020-03-25" @default.
- W3003335752 modified "2023-10-17" @default.
- W3003335752 title "Room Temperature Coupling of Aryldiazoacetates with Boronic Acids Enhanced by Blue Light Irradiation" @default.
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- W3003335752 doi "https://doi.org/10.1002/chem.201905812" @default.
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