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- W3004621746 abstract "The direct pyrolysis of metal organic frameworks (MOFs) has recently provided an effective method to prepare various metal-incorporated composite carbon materials. In this work, hierarchical Co-embedded N-doped porous carbon microspheres were synthesized by controlled pyrolysis of bimetallic Zn-Co Prussian blue analogues (PBAs), in which the metallic Zn component served as thermally removable template and ligand [Co(CN)6]3− served as both Co and N sources. When devoted to catalyzing the reduction of 4-nitrophenol (4-NPh) into 4-aminophenol (4-APh), the optimized catalyst exhibited a large apparent rate constant of 1.35 min−1 and high turnover frequency (TOF) of 0.0204 s−1, which was superior to the majority of noble-metal-based catalysts. Besides, a home-made continuous flow catalysis system was readily constructed. Control experiments confirmed that both partially uncovered and totally in-built active metallic Co species acted as catalytically active sites. This work might provide a further understanding of the identification of active sites within metal-incorporated carbon-based catalysts." @default.
- W3004621746 created "2020-02-14" @default.
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- W3004621746 date "2020-05-01" @default.
- W3004621746 modified "2023-10-16" @default.
- W3004621746 title "Hierarchical nitrogen-doped porous carbon incorporating cobalt nanocrystal sites for nitrophenol reduction" @default.
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- W3004621746 doi "https://doi.org/10.1016/j.ces.2020.115525" @default.
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