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• W3005689968 startingPage "1760" @default.
• W3005689968 abstract "The catalytic C(sp3)–H functionalization is highly desirable yet challenging in organic synthesis. Incorporation of the SP(O)(OR)2 group through C(sp3)–H functionalization remains unexplored. We herein report an unprecedented protocol for phosphorothiolation of primary and secondary C(sp3)–H via a multicomponent reaction with N-fluoro-substituted amides, elemental sulfur, and P(O)H compounds involving a sequence of amidyl radical generation, 1,5-HAT, and a Cu-catalyzed cross coupling of the resulting carbon radical with (RO)2P(O)SH (generated in situ)." @default.
• W3005689968 created "2020-02-24" @default.
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• W3005689968 date "2020-02-13" @default.
• W3005689968 modified "2023-10-14" @default.
• W3005689968 title "Copper-Catalyzed Remote C(sp³)–H Phosphorothiolation of Sulfonamides and Carboxamides in a Multicomponent Reaction" @default.
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• W3005689968 doi "https://doi.org/10.1021/acs.orglett.0c00044" @default.
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