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• W3005981943 abstract "The alkali-metal molybdate iodate Na3(MoO4)(IO3) (I) and mixed-alkali-metal fluoromolybdate Na3Cs(MoO2F4)2 (II) were obtained via a mild hydrothermal reaction using a Teflon-pouch method. I crystallizes in the triclinic space group P1, whose structure comprises a 3D backbone made up of isolated [IO3]- pyramids and [MoO4]2- tetrahedra connected via 5- and 6-fold coordinated sodium cations. II crystallizes in the monoclinic space group P21/c and comprises isolated [MoO2F4]2- octahedra with strong out-of-center distortions and the Na+ as well as Cs+ cations acting as interstitial ions. Both compounds have been characterized by infrared (IR) spectra and ultraviolet-visible-near-infrared (UV-vis-NIR) diffuse reflectance spectra. First-principles calculations respectively reveal that they exhibit birefringence values with Δn = 0.078 and 0.210 at 1064 nm for I and II, and the origin of the birefringence is discussed." @default.
• W3005981943 created "2020-02-24" @default.
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• W3005981943 date "2020-02-13" @default.
• W3005981943 modified "2023-10-15" @default.
• W3005981943 title "Structural Diversity of Molybdate Iodate and Fluoromolybdate: Syntheses, Structures, and Calculations on Na₃(MoO₄)(IO₃) and Na₃Cs(MoO₂F₄)₂" @default.
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• W3005981943 doi "https://doi.org/10.1021/acs.inorgchem.9b03383" @default.
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