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• W3006361415 abstract "Two approaches to a 1-aryl-4-trifluoromethyltriazole are described. Initially, a late-stage trifluoromethylation of the corresponding 1-aryl-4-iodotriazole using methyl fluorosulfonyldifluoroacetate (MDFA) was employed. However, the reaction was fraught with several safety and operational challenges, primarily due to the evolution of ∼33 equiv of gas per equiv of substrate. While some of these challenges were either addressed or mitigated through operations in plug flow, the process remained low yielding and suboptimal. Subsequently, a more convergent, longer-term route involving a Cu-mediated decarboxylative Click reaction was developed." @default.
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• W3006361415 date "2020-02-10" @default.
• W3006361415 modified "2023-09-27" @default.
• W3006361415 title "Two Approaches to a Trifluoromethyl Triazole: A Fit-for-Purpose Trifluoromethylation in Flow-Mode and a Long-Term Decarboxylative Click Approach" @default.
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• W3006361415 doi "https://doi.org/10.1021/acs.oprd.9b00492" @default.
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