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• W3007183003 endingPage "104812" @default.
• W3007183003 startingPage "104812" @default.
• W3007183003 abstract "Designing an efficient catalyst for the selective oxidation of biomass-derived platform chemical to value-added chemicals has always been an emerging field in the scientific community as well as for the industrial applications. Here, in the present study, the efforts were directed towards the development of catalyst based on non-precious metals for the selective oxidation of platform chemical, 5-hydroxymethylfurfural (5-HMF) to value-added chemical, 5-Formyl Furan-2-Carboxylic Acid (FFCA). Mixed metal oxide-based catalysts-containing manganese (Mn) and iron (Fe) with different wt% (MnxFey; x: y = 9:1, 7:3, 5:5, 3:7, 1:9) were successfully synthesized via hydrothermal route. The catalytic results showed the best yield of 37.7 % FFCA with 83.0 % conversion of 5-HMF using Mn3Fe7 under optimised reaction conditions (0.5 mmol Na2CO3, 140 °C, 90 min and 30 bar O2). The characterizations through various techniques such as X-ray Diffractometer (XRD), Scanning Electron Microscope (SEM) and Energy-Dispersive X-ray Spectroscopy (EDS) suggested that the synthesised mixed oxides catalysts are composed of MnO2, MnCO3 and Fe2O3 phases with uniform distribution throughout the catalyst. Thus, the synergic effect of these mixed phases might play a role in selective oxidation of 5-HMF to FFCA. The influence of other reaction parameters such as time, temperature, pressure, the basicity and catalyst loading was also optimized for enhancing the yield of the oxidised product. The recyclability study revealed that Mn3Fe7 was stable for at least four runs in terms of FFCA yield." @default.
• W3007183003 created "2020-03-06" @default.
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• W3007183003 date "2020-06-01" @default.
• W3007183003 modified "2023-09-25" @default.
• W3007183003 title "Oxidation of 5-hydroxymethylfurfural to 5-formyl furan-2-carboxylic acid by non-precious transition metal oxide-based catalyst" @default.
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• W3007183003 doi "https://doi.org/10.1016/j.supflu.2020.104812" @default.
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