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• W3007242802 startingPage "1222" @default.
• W3007242802 abstract "Three bis‐chelates of indium(III) with (partially fluorinated) S,N,S ‐tridentate thiosemicarbazones (H 2 L) were prepared and their structures were studied in solution and in the solid state by NMR, ESI MS and single‐crystal X‐ray diffraction. The three compounds are isostructural in solution with five‐coordinate In III ions and two differently coordinated thiosemicarbazonato ligands, [In(L)(HL)]. A temperature‐dependent 1 H NMR study reflects the presence of dynamic processes in the molecules such as the resolution of hindered rotation around CN bonds with partial double‐bond character and the pH‐triggered isomerization between 5‐ and 6‐coordinate species. The latter is confirmed by the isolation of compounds with different solid‐state structures, [In(L)(HL)] and [In(L) 2 ] – , depending on fluorine‐substitutions in the periphery of the thiosemicarbazones." @default.
• W3007242802 created "2020-03-06" @default.
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• W3007242802 date "2020-03-12" @default.
• W3007242802 modified "2023-10-18" @default.
• W3007242802 title "Trigonal‐Bipyramidal vs. Octahedral Coordination in Indium(III) Complexes with Potentially <i>S,N,S</i> ‐Tridentate Thiosemicarbazones" @default.
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• W3007242802 doi "https://doi.org/10.1002/ejic.201901356" @default.
• W3007242802 hasPublicationYear "2020" @default.
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