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- W3007665086 abstract "Abstract GLC method has been developed for the quantitation of ammonium glycyrrhizinate as the aglycone, glycyrrhetic acid. The aglycone is freed from the sugar moiety in a dioxanewater mixture, using a well established acid hydrolysis procedure. The hydrolysate is extracted with chloroform, an aliquot is dried on a steam bath, and the residue is treated with pyridine - trimethylchlorosilane - N,0 - bis (trimethylsilyl)acetamide reagent. The reacted product and internal standard are then chromatographed on a column of 1.5% OV-1 on Gas Chrom Q. Recoveries from both water and sodas containing caramel averaged 87%." @default.
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- W3007665086 date "1970-07-01" @default.
- W3007665086 modified "2023-10-17" @default.
- W3007665086 title "Quantitation of Ammonium Glycyrrhizinate by Gas-Liquid Chromatography of the Silyl Ether Ester Derivative of the Aglycone" @default.
- W3007665086 doi "https://doi.org/10.1093/jaoac/53.4.698" @default.
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