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- W3007947719 endingPage "100209" @default.
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- W3007947719 abstract "In this study, we have developed a new method to synthesize mesoporous titanium silicalite-1 (TS-1) with a higher content of active titanium in the framework (more than 5%) than that obtained from the conventional hydrothermal synthesis. The new method combines two methods as follows: (1) a sol-gel method in tetrahydrofuran for the synthesis of TiO2–SiO2 composite with highly dispersed Ti species and (2) a dry gel conversion method for the crystallization to TS-1. This investigation revealed that the dispersion of Ti in the starting materials was quite important to synthesize mesoporous TS-1 with high content of Ti besides dry conversion method. The obtained mesoporous TS-1 with a high content of titanium showed higher catalytic activity in 1-hexene epoxidation than conventional TS-1. This high activity is likely to originate from the high content of titanium in the framework." @default.
- W3007947719 created "2020-03-06" @default.
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- W3007947719 date "2020-06-01" @default.
- W3007947719 modified "2023-09-26" @default.
- W3007947719 title "Synthesis of titanium silicalite-1 (TS-1) zeolite with high content of Ti by a dry gel conversion method using amorphous TiO2–SiO2 composite with highly dispersed Ti species" @default.
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- W3007947719 doi "https://doi.org/10.1016/j.mtchem.2019.100209" @default.
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