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- W3007950691 abstract "In this paper we report an effortless, convenient and less hazardous route for the synthesis of two Cu(II) complexes of phenol based 24- and 28-membered macrocyclic Schiff bases, [Se 2 {(CH 2 ) n N = C PhC 6 H 2 (OH)(4-CH 3 )PhC = N(CH 2 ) n } 2 ] (where n = 2, L a H 2 ; n = 3, L b H 2 ) of Se 2 N 4 O 2 type. These ligands on coordination with Cu(CH 3 COO) 2 ·H 2 O in 1:2 M ratio in methanol gave mononuclear complexes [Se{(CH 2 ) n N = CPhC 6 H 2 (O)(4-CH 3 )PhC = O} 2 Cu] (n = 2, 1 ; n = 3, 2 ) with the loss of bis(aminoalkyl)selenide and acetic acid. In both of these complexes, two imine (C = N) bonds of the ligand molecule undergo hydrolysis, and links with Cu(II) in tetradentate ( N 2 O 2 ) fashion. The selenium atom does not form part of the copper(II) coordination sphere. The complexes ( 1 and 2 ) have been characterized by elemental analyses, conductivity measurements, mass spectrometry, IR, electronic, 1 H, 13 C{ 1 H} and 77 Se{ 1 H} NMR spectroscopy and cyclic voltammetry." @default.
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- W3007950691 date "2021-01-01" @default.
- W3007950691 modified "2023-10-16" @default.
- W3007950691 title "Cu(II) complexes of selenium bearing Se2N4O2 macrocyclic Schiff bases: Synthesis and electrochemical studies" @default.
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- W3007950691 doi "https://doi.org/10.1016/j.matpr.2020.01.577" @default.
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