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- W3008202819 endingPage "2617" @default.
- W3008202819 startingPage "2610" @default.
- W3008202819 abstract "Abstract A volatile organic solvent‐free deep eutectic solvent (DES) was prepared by utilizing 1 : 10 ratio of potassium carbonate (PC) as a hydrogen bond acceptor (HBA) and ethylene glycol (EG) as a hydrogen bond donor (HBD). Subsequently, DES was utilized as a solvent in the Pd‐catalyzed Suzuki‐Miyaura or Sonogashira cross‐coupling reactions of boronic acids or acetylenes respectively with in situ generated 2‐bromobenzo[2,3][1,4]oxazepino[7,6‐b]quinoline, 3 The anhydrous conditions without air exclusion, low catalyst loading, low toxicity, high efficiency, low cost, and bioavailability are the advantages of DES in C−C bond forming reactions. Moreover, a gram‐scale reaction under mild conditions with an excellent yield was productive. The one‐pot reaction of 6‐bromo‐2‐chloroquinoline‐3‐carbaldehyde, 1 through 2‐bromobenzo [2,3][1,4]oxazepino [7,6‐b]quinoline, 3 intermediate, and subsequent Suzuki‐Miyaura or Sonogashira coupling was successfully attempted." @default.
- W3008202819 created "2020-03-06" @default.
- W3008202819 creator A5027441415 @default.
- W3008202819 creator A5045804521 @default.
- W3008202819 date "2020-02-27" @default.
- W3008202819 modified "2023-09-26" @default.
- W3008202819 title "A Base‐Free Pd‐Precatalyst Mediated Suzuki‐Miyaura and Sonogashira Cross‐Coupling in Deep Eutectic Solvents" @default.
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- W3008202819 doi "https://doi.org/10.1002/slct.202000276" @default.
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