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- W3008554561 abstract "Abstract Three methods for the extraction and derivatization of alcohols, carbox j lie acids, and phenols from airborne particulates were compared and evaluated. Derivatization of the sample during ultrasonic agitation to form trimethylsilyl derivatives increased the recovery of reactive oxygenated hydrocarbons compared to the standard method of extraction followed by derivatization. A single solvent, methylene chloride, with a strong and volatile silylating reagent, N,0- bis(trimethylsilyl)trifluoroacetamide, extracted a large number of reactive components with a minimum of interference. When the extraction/derivatization procedure was repeated 4 or more times for a total extraction time of at least 30 h, greater than 90% of the major mono- and difunctional group-containing components was recovered" @default.
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- W3008554561 date "1987-09-01" @default.
- W3008554561 modified "2023-09-27" @default.
- W3008554561 title "Simultaneous Ultrasonic Extraction and Silylation for Determination of Organic Acids, Alcohol, and Phenols from Airborne Particulate Matter" @default.
- W3008554561 doi "https://doi.org/10.1093/jaoac/70.5.897" @default.
- W3008554561 hasPublicationYear "1987" @default.
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