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- W3010807539 endingPage "151823" @default.
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- W3010807539 abstract "A visible light-mediated (blue LED: λ = 455 ± 10 nm), rose bengal-catalyzed intramolecular cycloaromatization reaction of alkyl 1, 1′-biaryl-2-ones for the synthesis of 10-alkylphenanthren-9-ols in water under open air atmosphere at ambient conditions has been developed. Experimental studies demonstrate that the reaction proceeded via a radical pathway. This protocol is applicable to a wide variety of substrates giving expected 10-alkylphenanthren-9-ols in good yields, appropriate for the gram-scale synthesis, atom economy, and eco-friendly as compared to literature reported methodology for the preparation of phenanthrol derivatives. Moreover, to the best of our knowledge, no instance has hitherto been accounted on the visible light-induced transformation of readily available alkyl 1,1′-biaryl-2-ones to 10-alkylphenanthren-9-ols." @default.
- W3010807539 created "2020-03-23" @default.
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- W3010807539 date "2020-04-01" @default.
- W3010807539 modified "2023-09-26" @default.
- W3010807539 title "Visible light-mediated, rose Bengal-catalyzed oxidative radical C H cyclization of alkyl 1,1′-biaryl-2-ones: An efficient synthesis of 10-alkylphenanthren-9-ols in water" @default.
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- W3010807539 doi "https://doi.org/10.1016/j.tetlet.2020.151823" @default.
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