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- W3010953418 abstract "Multidentate, soft-Lewis basic, complexant scaffolds have displayed significant potential in the discrete speciation of the minor actinides from the neutron-absorbing lanthanides resident in spent nuclear fuel. Efforts to devise convergent synthetic strategies to targets of interest to improve liquid-liquid separation outcomes continue, but significant challenges to improve solubility in process-relevant diluents to effectively define meaningful structure-activity relationships remain. In the current work, a synthetic method to achieve the challenging 2,2'-bipyridine bond of the bis-1,2,4-triazinyl-2,2'-bipyridine (BTBP) complexant class leveraging a Pd-catalyzed Ullman-type coupling is reported. This convergent strategy improves upon earlier work focused on linear synthetic access to the BTBP complexant moiety. Method optimization, relevant substrate scope and application, as well as a preliminary mechanistic interrogation are reported herein." @default.
- W3010953418 created "2020-03-23" @default.
- W3010953418 creator A5019118619 @default.
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- W3010953418 date "2020-01-01" @default.
- W3010953418 modified "2023-09-24" @default.
- W3010953418 title "Convergent access to bis-1,2,4-triazinyl-2,2′-bipyridines (BTBPs) and 2,2′-bipyridines <i>via</i> a Pd-catalyzed Ullman-type reaction" @default.
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- W3010953418 doi "https://doi.org/10.1039/d0ra00673d" @default.
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