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- W3012165481 abstract "To obtain high-capacity electrode materials and meanwhile actualize the reuse of scrap lead paste, a novel alkylamine-mediated thermolysis route is proposed herein for one-pot preparation of high-quality PbO nanomaterials, relying on the thermal decomposition of lead carboxylate in hot solvent in the presence of hexadecylamine (HDA). This synthetic route allows us to produce uniform PbO nanowires with a diameter of 7.1 nm and a length beyond 10 μm, and nanosheets and nanorings with a lateral size of ca. 310 nm on a gram scale, by simply tuning the alkylamine content or reaction time. In particular, we have employed various means to unveil the key role of HDA, i.e., precursor activation and surface passivation function, in the controlled preparation of such PbO nanomaterials. Impressively, when serving as the positive active materials for lead acid batteries (LABs), the anodes based on PbO nanowires displayed an excellent discharge performance: its discharge capacity and active material utilization ratios could reach 164.3 mA h/g and 68.5% respectively even at a discharge current density as high as 50 mA/g, which are superior to most of the previously-reported values. Such an excellent discharge performance was speculated to result from the synergization effect of the large ECSA, small charge transfer resistance and highly active exposed facets associated with the PbO nanowires." @default.
- W3012165481 created "2020-03-23" @default.
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- W3012165481 date "2020-08-01" @default.
- W3012165481 modified "2023-10-15" @default.
- W3012165481 title "One-pot and high-yield preparation of ultrathin β-PbO nanowires and nanosheets for high-capacity positive electrodes in lead-acid batteries" @default.
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- W3012165481 doi "https://doi.org/10.1016/j.jallcom.2020.154845" @default.
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