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• W3013720710 startingPage "11113" @default.
• W3013720710 abstract "Abstract Crystalline 1,4‐distannabarrelene compounds [(ADC Ar ) 3 Sn 2 ]SnCl 3 ( 3 ‐ Ar ) (ADC Ar ={ArC(NDipp) 2 CC}; Dipp=2,6‐ i Pr 2 C 6 H 3 , Ar=Ph or DMP; DMP=4‐Me 2 NC 6 H 4 ) derived from anionic dicarbenes Li(ADC Ar ) ( 2 ‐ Ar ) (Ar=Ph or DMP) have been reported. The cationic moiety of 3 ‐ Ar features a barrelene framework with three coordinated Sn II atoms at the 1,4‐positions, whereas the anionic unit SnCl 3 is formally derived from SnCl 2 and chloride ion. The all carbon substituted bis‐stannylenes 3 ‐ Ar have been characterized by NMR spectroscopy and X‐ray diffraction. DFT calculations reveal that the HOMO of 3 ‐ Ph ( ϵ =−6.40 eV) is mainly the lone‐pair orbital at the Sn II atoms of the barrelene unit. 3 ‐ Ar readily react with sulfur and selenium to afford the mixed‐valence Sn II /Sn IV compounds [(ADC Ar ) 3 SnSn(E)](SnCl 6 ) 0.5 (E=S 4 ‐ Ar , Ar=Ph or DMP; E=Se 5 ‐ Ph )." @default.
• W3013720710 created "2020-04-03" @default.
• W3013720710 creator A5004486193 @default.
• W3013720710 creator A5009050687 @default.
• W3013720710 creator A5029807989 @default.
• W3013720710 creator A5043938107 @default.
• W3013720710 creator A5052372563 @default.
• W3013720710 date "2020-07-28" @default.
• W3013720710 modified "2023-10-14" @default.
• W3013720710 title "Distannabarrelenes with Three Coordinated Sn ^II Atoms" @default.
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