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• W3016565011 abstract "Abstract A new chiral open‐tubular capillary electrochromatography column was prepared with 6‐O‐monotosyl‐deoxy‐β‐cyclodextrin as staionary phase by covalent immobilization on inner wall of a fused‐silica capillary. Preparation procedure of the open‐tubular column was investigated and resulting surface morphology was determined using scanning electron microscopy. Moreover, the enantiomeric separation performance of open‐tubular capillary electrochromatography column was evaluated by using several related benzimidazoles as model analytes, including pantoprazole, tenatoprazole, omeprazole, and lansoprazole. The primary factors affecting its separation efficiency, such as type, concentration, and pH of buffer, applied voltage were optimized. In the optimum conditions, the enantiomers of four analytes revealed high resolutions of 5.75–8.83. The relative standard deviation values for the migrated times and resolutions of the model analyte representing intraday, interday, and column‐to‐column were less than 1.8 and 1.3%, respectively. The chiral open‐tubular capillary electrochromatography column still had satisfactory separation performance after continuous use for 72 h or intermittent use for 3 months." @default.
• W3016565011 created "2020-04-24" @default.
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• W3016565011 date "2020-04-16" @default.
• W3016565011 modified "2023-10-18" @default.
• W3016565011 title "Preparation of open‐tubular CEC column bonded with 6‐O‐monotosyl‐deoxy‐β‐cyclodextrin and its application in the enantioseparation of several related benzimidazoles" @default.
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• W3016565011 doi "https://doi.org/10.1002/sscp.202000014" @default.
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