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• W3017598650 abstract "The clinical aminoglycoside antibiotic gentamicin is a mixture of several difficult-to-separate major and minor components. The relative inaccessibility of the minor components in particular complicates efforts to separate antibacterial activity from nephro- and/or ototoxicity and to clarify the origin of the potentially therapeutically important read-through activity. With a view to facilitating such studies, the synthesis of a fully and selectively protected garamine-based acceptor has been developed from readily available sisomicin. Glycosylation of this acceptor with a 6-azido-6,7-dideoxy-d-glycero-d-glucoheptopyranosyl donor affords gentamicin B1 after deprotection, whereas employment of a 2-azido-2-deoxy-d-glucopyranosyl donor under N,N-dimethylformamide-directed glycosylation conditions affords gentamicin X2 after deprotection." @default.
• W3017598650 created "2020-05-01" @default.
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• W3017598650 date "2020-04-28" @default.
• W3017598650 modified "2023-10-18" @default.
• W3017598650 title "Synthesis of Gentamicin Minor Components: Gentamicin B1 and Gentamicin X2" @default.
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• W3017598650 doi "https://doi.org/10.1021/acs.orglett.0c01107" @default.
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