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• W3018029541 endingPage "125164" @default.
• W3018029541 startingPage "125164" @default.
• W3018029541 abstract "Abstract Chemical fixation of carbon dioxide (CO2) is among the fundamental pathways to considerably decrease its accumulation in the atmosphere. Herein, we present utilization of glucose, oxalic acid and urea to derive carbonaceous materials for chemical fixation of CO2 with an epoxide into cyclic carbonate without the aid of solvent. The derived heterogeneous carbonaceous materials containing different carboxyl, hydroxyl and amines were developed by facile and straightforward hydrothermal method and used with a certain amount of KI which acts as cocatalyst. The synthesized catalysts such as Glucose Carbonaceous Material (GCM), Oxalic-Glucose Carbonaceous Material (O-GCM) and Urea-Glucose Carbonaceous Material (U-GCM) were characterized by FT-IR, XRD, TGA, BET, TPD, SEM and XPS. The catalytic properties were evaluated by varying different reaction parameters, including the amount of catalyst, temperature, pressure, and time. The results show that the catalyst has excellent catalytic performance under the mild reaction conditions with outstanding stability owing to easy separation from the reaction mixture. Moreover, results demonstrate that the catalyst has shown superior catalytic activity due to the presence of amine ( NH), hydroxyl ( OH) and carboxylic ( COOH) enriched carbonaceous framework which enables synergistic effect to considerably enhance the catalytic performance." @default.
• W3018029541 created "2020-05-01" @default.
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• W3018029541 date "2020-09-01" @default.
• W3018029541 modified "2023-10-18" @default.
• W3018029541 title "Chemical fixation of carbon dioxide catalyzed via hydroxyl and carboxyl-rich glucose carbonaceous material as a heterogeneous catalyst" @default.
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• W3018029541 doi "https://doi.org/10.1016/j.cej.2020.125164" @default.
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