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• W3019510360 abstract "Abstract The modified TiO 2 nanoparticles (TiO 2 NPs) with diblock copolymer were successfully synthesized via surface‐initiated atom transfer radical polymerization (SI‐ATRP). The modified TiO 2 contained the ‐NH 2 group (TiO 2 ‐APTES) was obtained by 3‐aminopropyltriethoxysilane (APTES) as a coupling agent. Bromine modified TiO 2 NPs (TiO 2 ‐Br), the ATRP initiator was prepared by the reaction of ‐NH 2 in TiO 2 ‐APTES with 2‐bromoisobutyryl bromide (BiBB). The block copolymer of the polyacrylonitrile and poly(hydroxyethyl acrylate) (PAN‐b‐PHEA) on the TiO 2 surface was synthesized with TiO 2 ‐Br as initiator via ATRP. The differential scanning calorimetry (DSC) analysis revealed two Tg values corresponding to two blocks, which indicated two polymer chains of the modified TiO 2 . The result of Gel Permeation Chromatography (GPC) shown increasing molecular weight of the PAN‐b‐PHEA also demonstrated the block copolymer structure." @default.
• W3019510360 created "2020-05-01" @default.
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• W3019510360 date "2020-04-21" @default.
• W3019510360 modified "2023-09-25" @default.
• W3019510360 title "Synthesis of Modified TiO ₂ Nanoparticles with Polyacrylonitrile and Poly(hydroxyethyl acrylate) via ATRP" @default.
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• W3019510360 doi "https://doi.org/10.1002/slct.202000134" @default.
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