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• W3019679108 abstract "Bi 5 Ti 3 FeO 15 (pentabismuth trititanium iron pentadecaoxide), which is a multiferroic four-layer Aurivillius phase compound, has received much attention in recent years. However, three mutually inconsistent orthorhombic space groups, i.e. A 2 1 am , Fmm 2 and Pnn 2, have been reported for the room-temperature phase of Bi 5 Ti 3 FeO 15 by X-ray and neutron diffraction investigations. Here, electron diffraction results are presented and discussed for the first time to unambiguously clarify the room-temperature space group of ceramic Bi 5 Ti 3 FeO 15 . It has been found that all the observed reflections from the ceramic agree with those expected in A 2 1 am , while the observed reflections 011, 013 and 015 should be forbidden in the case of Fmm 2, and no 107 and 109 reflections were observed although allowed for Pnn 2. The present study has demonstrated that the space group of Bi 5 Ti 3 FeO 15 ceramic is A 2 1 am rather than Fmm 2 or Pnn 2, an identification that proved to be a challenge for X-ray diffraction. On the basis of the space group A 2 1 am , the lattice parameters of the Bi 5 Ti 3 FeO 15 ceramic were calculated from its X-ray diffraction data." @default.
• W3019679108 created "2020-05-01" @default.
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• W3019679108 date "2020-04-20" @default.
• W3019679108 modified "2023-10-16" @default.
• W3019679108 title "Electron diffraction study of the space group of Bi₅Ti₃FeO₁₅ multiferroic ceramic" @default.
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• W3019679108 doi "https://doi.org/10.1107/s2053229620005045" @default.
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