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• W3021799449 abstract "Herein we report a selective DIBAL-H-mediated reduction of a heterocyclic diester to the corresponding monoaldehyde using continuous flow chemistry. The use of continuous flow enabled operation at lower temperatures and better control of the reaction time, thereby allowing for a significant increase in reaction selectivity and yield compared with batch conditions. The reaction’s development as a continuous flow process and its scale-up from laboratory gram scale to multikilogram scale are discussed, including design of experiments studies to probe the optimal reaction window." @default.
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• W3021799449 date "2020-05-08" @default.
• W3021799449 modified "2023-10-11" @default.
• W3021799449 title "Selective DIBAL-H Monoreduction of a Diester Using Continuous Flow Chemistry: From Benchtop to Kilo Lab" @default.
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• W3021799449 doi "https://doi.org/10.1021/acs.oprd.0c00158" @default.
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