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• W3022151431 startingPage "2298" @default.
• W3022151431 abstract "The translation of olefin metathesis reactions from the laboratory to process scale has been challenging with traditional batch techniques. In this contribution, we describe a continuous membrane reactor design that selectively permeates the ethylene byproduct from metathetical processes, thereby overcoming the mass-transport limitations that have negatively influenced the efficiency of this transformation in batch vessels. The membrane sheet-in-frame pervaporation module yielded turnover numbers of >7500 in the case of diethyl diallylmalonate ring-closing metathesis. The preparation of more challenging, low-effective-molarity substrates, a cyclooctene and a 14-membered macrocyclic lactone, was also effective. A comparison of optimal membrane reactor conditions to a sealed tubular reactor revealed that the benefits of ethylene removal are most apparent at low reaction concentrations." @default.
• W3022151431 created "2020-05-13" @default.
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• W3022151431 date "2020-05-01" @default.
• W3022151431 modified "2023-09-27" @default.
• W3022151431 title "A Scalable Membrane Pervaporation Approach for Continuous Flow Olefin Metathesis" @default.
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• W3022151431 doi "https://doi.org/10.1021/acs.oprd.0c00061" @default.
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