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- W3022496105 abstract "This study presents a novel preconcentration and separation method for manganese determination using a green switchable solvent-based liquid-phase microextraction and slotted quartz tube-flame atomic absorption spectrometry (SS-LPME-SQT-FAAS). The switchable solvent was prepared from the mixture of N,N dimethylamine and ultrapure water, using dry carbon dioxide for protonation. A coordinate complex of manganese was formed with ((E)-2,4-dibromo-6-(((3-hydroxyphenyl)imino)methyl)phenol ligand synthesized in the lab. Parameters including pH, buffer volume, ligand concentration/volume, switchable solvent volume and sodium hydroxide concentration/volume were optimized to enhance complex formation and extraction efficiency. The limit of detection (LOD), limit of quantification (LOD) and enrichment factor were determined as 0.71 µg L−1, 2.4 µg L−1 and 101 folds, respectively. The applicability of the developed method was tested in soil samples using the matrix matching calibration method. The percent recovery results obtained (98–105%) established the method’s accuracy and applicability to real samples." @default.
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- W3022496105 date "2020-09-01" @default.
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- W3022496105 title "Determination of trace manganese in soil samples by using eco-friendly switchable solvent based liquid phase microextraction-3 holes cut slotted quartz tube-flame atomic absorption spectrometry" @default.
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- W3022496105 doi "https://doi.org/10.1016/j.microc.2020.104981" @default.
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