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• W3023313426 abstract "A P(NMe2)3-mediated annulation reaction of N-acyldiazenes with isothiocyanates, producing 2-imino-1,3,4-thiadiazoles, is reported. This reaction proceeds well with crude N-acyldiazenes derived from the oxidation of hydrazides by iodine and permits the sequential synthesis of products directly from hydrazides without purification of the less stable N-acyldiazene intermediates. The reaction does not require transition metals and is a simple, scalable operation with broad substrate scope." @default.
• W3023313426 created "2020-05-13" @default.
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• W3023313426 date "2020-05-11" @default.
• W3023313426 modified "2023-10-16" @default.
• W3023313426 title "Synthesis of 2-Imino-1,3,4-thiadiazoles from Hydrazides and Isothiocyanates via Sequential Oxidation and P(NMe₂)₃-Mediated Annulation Reactions" @default.
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• W3023313426 doi "https://doi.org/10.1021/acs.orglett.0c01393" @default.
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