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• W3023604197 abstract "Abstract The synthesis of a series of 4-aza cross-conjugated cyclopentenones, inspired by the natural prostaglandin Δ12,14-15-deoxy-PGJ2 (5) is described. Using the 4-aza cyclopentenone 7, the installation of the α-side chain was performed using N-functionalisation, following a Boc-deprotection. The ω-side chain was then installed through a Baylis-Hillman type aldol reaction with trans-2-octenal. This afforded 11, the aza-analogue of 5. With this prostaglandin analogue in hand, a series of thiol adducts (14–16) were prepared. Included are activities for compounds 11 and 14–16 in relation to inhibition of the transcription factor NF-κB." @default.
• W3023604197 created "2020-05-13" @default.
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• W3023604197 date "2020-06-01" @default.
• W3023604197 modified "2023-09-24" @default.
• W3023604197 title "Synthesis of the 4-aza cyclopentenone analogue of Δ12,14-15-deoxy-PGJ2 and S-cysteine adducts" @default.
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• W3023604197 doi "https://doi.org/10.1016/j.tetlet.2020.151969" @default.
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