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- W3023958598 abstract "Publisher SummarySulfur compounds are chemical compounds that contain the chemical element sulfur. This chapter discusses the gas chromatography separation of hydrogen sulfide, carbonyl sulfide, sulfur dioxide, and methylmercaptan. Mass spectra of aliphatic thiols, thioethers, aromatic thiols and isothiocyanates are determined. The presence of sulfur can be detected by the 34S isotope (4.4% per atom of S) and the large mass defect of sulfur in accurate mass measurements. The mass spectra of cyclic thioethers exhibit intense M+• peaks and an intense fragment ion peak due to a double homolytic cleavage. Fragmentation of thioethers is analogous to the fragmentation of aliphatic ethers. The M+• peak in the mass spectra of thioesters is more intense than that of the corresponding oxygenated esters." @default.
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- W3023958598 date "2011-01-01" @default.
- W3023958598 modified "2023-09-26" @default.
- W3023958598 title "Sulfur Compounds" @default.
- W3023958598 doi "https://doi.org/10.1016/b978-0-12-373628-4.00036-8" @default.
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