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• W3024842893 abstract "Abstract A comprehensive model is developed for polycondensation of 1,3‐propanediol in a batch reactor. The model accounts for formation, consumption, and evaporation of cyclic oligomers. Measurements of species and end‐group concentrations in the reactor and collected condensate are used to estimate 36 kinetic and mass‐transfer parameters. The model and parameter estimates provide good fits to cyclic‐oligomer data obtained using four different levels of super‐acid catalyst. Predictions from the model reveal that end‐biting reactions are important for formation of cyclic oligomers during early stages of each batch‐reactor run, whereas back‐biting reactions become important at longer reaction times. Simulation results reveal that ring‐opening polyaddition reactions contribute significantly to growth of polymer chains at long reaction times." @default.
• W3024842893 created "2020-05-21" @default.
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• W3024842893 date "2020-05-17" @default.
• W3024842893 modified "2023-09-26" @default.
• W3024842893 title "An Improved PO3G Model–Accounting for Cyclic Oligomers" @default.
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• W3024842893 doi "https://doi.org/10.1002/mats.202000023" @default.
• W3024842893 hasPublicationYear "2020" @default.
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