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• W3025237054 abstract "Single crystals of cadmium pentaoxidoditellurate(IV), CdTe 2 O 5 , were obtained as by-products in a hydrothermal reaction of Cd(NO 3 ) 2 ·4H 2 O, TeO 2 , H 6 TeO 6 and NH 3 (molar ratios 2:1:1:6) at 483 K for seven days. The crystals represent a different polymorph (henceforth referred to as the β -form) than the α -CdTe 2 O 5 crystals grown from the melt, and are isotypic with hydrothermally grown ∊ -CaTe 2 O 5 . The asymmetric unit of β -CdTe 2 O 5 comprises one Cd, two Te and five O sites, all of which are located in general positions (Wyckoff position 4 e ). The cadmium(II) atom is coordinated by seven oxygen atoms, forming 2 ∞ [CdO 6/2 O 1/1 ] (100) layers. Both tellurium sites are surrounded by four oxygen atoms with one of them being at a significantly longer distance than the other three. The resulting bisphenoidal [TeO 4 ] units also form layers propagating parallel to (100) by sharing edges with each other. The stereochemically active 5 s 2 lone pair of the Te IV atoms leads to the formation of large channels extending along [011] and smaller ones along [010]. A quantitative comparison between the crystal structures of β -CdTe 2 O 5 and ∊-CaTe 2 O 5 is made." @default.
• W3025237054 created "2020-05-21" @default.
• W3025237054 creator A5032283210 @default.
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• W3025237054 date "2020-05-15" @default.
• W3025237054 modified "2023-10-15" @default.
• W3025237054 title "The crystal structure of a new CdTe2O5 polymorph, isotypic with ∊-CaTe2O5" @default.
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• W3025237054 doi "https://doi.org/10.1107/s2056989020006283" @default.
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