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- W3025511115 abstract "Hierarchical iron-containing TS-1 zeolites (FTS) were successfully synthesized via post-treatment desilication over microporous Fe-TS-1, which were prepared through a one-step hydrothermal synthesis. The prepared samples were characterized by X-ray diffraction, N2 adsorption–desorption, field-emission scanning electron microscopy, transmission electron microscopy, Fourier transform infrared spectroscopy, ultraviolet visible spectroscopy, and X-ray fluorescence spectrometry. The experimental results illustrated that the MFI structure of all the FTS samples remained unchanged after NaOH desilication and acid treatment. The newly created mesopores can be controlled by changing the amount of framework Fe, as the extraction of Si could be affected because of the inhibitory effect of iron species during the desilication process. The catalytic performance of the prepared samples in phenol hydroxylation with H2O2 was investigated. Among all the samples, FTS-50-D showed a highest phenol conversion of 45.2% and a dihydroxybenzene selectivity of 95.2%. Besides, FTS-50-D also showed good reusability for five recycling tests." @default.
- W3025511115 created "2020-05-21" @default.
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- W3025511115 date "2020-05-13" @default.
- W3025511115 modified "2023-10-01" @default.
- W3025511115 title "Iron-Containing TS-1 Zeolites with Controllable Mesopores by Desilication and Their Application in Phenol Hydroxylation" @default.
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- W3025511115 doi "https://doi.org/10.1021/acs.iecr.0c00048" @default.
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