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- W3025653419 abstract "Crystal structures for a series of bis(acetylacetonato)oxovanadium(IV) complexes containing N -donor pyridyl ligands are reported, namely, bis(acetylacetonato-κ 2 O , O ′)oxido(pyridine-κ N )vanadium(IV), [V(C 5 H 7 O 2 ) 2 O(C 5 H 5 N)], 1 , bis(acetylacetonato-κ 2 O , O ′)oxido(pyridine-4-carbonitrile-κ N )vanadium(IV), [V(C 5 H 7 O 2 ) 2 O(C 6 H 4 N 2 )], 2 , and bis(acetylacetonato-κ 2 O , O ′)(4-methoxypyridine-κ N )oxidovanadium(IV), [V(C 5 H 7 O 2 ) 2 O(C 6 H 7 NO)], 3 , Compounds 1 – 3 have the formulae VO(C 5 H 7 O 2 ) 2 L , where L = pyridine ( 1 ), 4-cyano-pyridine ( 2 ), and 4-methoxypyridine ( 3 ). Compound 1 was previously reported [Meicheng et al. (1984). Kexue Tongbao , 29 , 759–764 and DaSilva, Spiazzi, Bortolotto & Burrow (2007). Acta Crystallogr. , E 63 , m2422] and redetermined here at cryogenic temperatures. Compounds 1 and 2 as pyridine and 4-cyanopyridine adducts, respectively, crystallize as distorted octahedral structures with the oxo and pyridyl ligands trans to one another. A crystallographic twofold axis runs through the O—V—N bonds. Compound 3 containing a 4-methoxypyridine ligand crystallizes as a distorted octahedral structure with the oxo and pyridyl ligands cis to one other, removing the twofold symmetry seen in the other complexes." @default.
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- W3025653419 date "2020-05-15" @default.
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- W3025653419 title "Crystal structures of a series of bis(acetylacetonato)oxovanadium(IV) complexes containing N-donor pyridyl ligands" @default.
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- W3025653419 doi "https://doi.org/10.1107/s2056989020006246" @default.
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