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• W3026202785 endingPage "113365" @default.
• W3026202785 startingPage "113365" @default.
• W3026202785 abstract "A selective detection strategy for salicylic acid (SA) based on the electrosorption/electrodesorption process using an electrochemically controlled solid phase extraction (EC-SPME) configuration is presented. We used conducting polymer polypyrrole (PPy) bearing the anionic dopant nitrate (PPy/nitrate) as a sorbent element for the extraction of SA in plasma and urine samples. The vertically grown nanosheets conducting film was directly synthesized by cyclic voltammetry method on a rod-shaped stainless steel electrode. The prepared electrode was employed for selective electrosorption of SA from sample solutions by applying positive potential and following its successive electrodesorption by the use of negative potential. Several parameters like synthesis conditions, anion dopant effect, potential and time of electrosorption/electrodesorption, and exchange anion type were explored to achieve the optimal conditions. The morphology of nanostructure PPy/nitrate sorbent was characterized by scanning electron microscopy (SEM). The electrosorption of SA was demonstrated by using FT-IR and fluorescence microscopic imaging. The obtained linear dynamic range (LDR), the limit of detection (LOD), and RSD% of SA determination by fluorescence spectrometry were 5–100 nanomol L−1, 1.4 nanomol L−1 and 4.9 (n = 5), respectively. The suggested technique was successfully applied for the quantification and determination of trace amounts of SA in biomedical samples without any additional treatment." @default.
• W3026202785 created "2020-05-29" @default.
• W3026202785 creator A5018381594 @default.
• W3026202785 creator A5023907260 @default.
• W3026202785 date "2020-09-01" @default.
• W3026202785 modified "2023-09-27" @default.
• W3026202785 title "Vertically grown nanosheets conductive polypyrrole as a sorbent for nanomolar detection of salicylic acid" @default.
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• W3026202785 doi "https://doi.org/10.1016/j.jpba.2020.113365" @default.
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• W3026202785 hasPublicationYear "2020" @default.
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