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- W3026708947 abstract "A Nickel Schiff base complex, insoluble in water, was synthesized and used as modifier. A Nickel Schiff base modified carbon paste electrode MCPE was build. The electrodes were characterized by scanning electron microscopy (SEM), energy dispersive X-Ray spectroscopy (EDXS), cyclic voltammetry and chronoamperometry. The modifier is elctroactive, a well defined redox couple of NiIII/NiII in alkaline medium was made in evidence. It presents a quasi-reversible system with electron transfer coefficient (0.38) and electron transfer rate of 4.5 s−1. The electrogenerated NiIII species on the surface of the electrode act as an excellent catalyst toward thiosulfate oxidation reaction with a chemical rate constant Kh equal to 23,6 M−1s−1. The different techniques involved in this study qualify our modified electrode as sensitive, reliable and very stable for thiosulfate analysis." @default.
- W3026708947 created "2020-05-29" @default.
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- W3026708947 date "2020-07-01" @default.
- W3026708947 modified "2023-10-17" @default.
- W3026708947 title "Elaboration of carbon paste electrode containing pentadentate Nickel-(II) Schiff base complex: Application to electrochemical oxidation of thiosulfate in alkaline medium" @default.
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- W3026708947 doi "https://doi.org/10.1016/j.arabjc.2020.05.007" @default.
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