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- W3029578916 abstract "Levels of serum sodium (Na) are widely determined in clinical laboratories. Accordingly, sodium quantification must be performed using reliable methods. Herein are reported the results of the evaluation of a new inductively coupled plasma mass spectrometry (ICP-MS) method for sodium quantification. Serum samples were diluted 100 × by 0.3% ultrapure nitric acid, and germanium (Ge) was used as an internal standard. Sodium calibration solutions with different concentrations were added to serum matrix solutions. The serum sodium concentration was calculated according to the standards addition method. The analytical performance of the method, as well as a comparison with other sodium method, was investigated. The correlation coefficients (r) between the measured Na/Ge ratios and the analyte concentration ratios were all > 0.9999. Intra- and between-assay coefficients of variation (CVs) were < 0.64% and < 0.57%, respectively, and the total CV was < 0.67%. The trueness of the method was verified by measuring a certified reference material, SRM 956d. The new ICP-MS method was compared with the 2017 and 2018 External Quality Assessment Scheme for Reference Laboratories in Laboratory Medicine (RELA). The results were well correlated with those obtained by the routine indirect ion selective electrode (ISE) method: sodium (ICP-MS, mmol/L) = 0.9895 × sodium (ISE, mmol/L) + 1.3049 (r = 0.9914, n = 40). The mean deviation between the results of the ICP-MS method and the indirect ISE method was –0.15%. The new ICP-MS method proved to be accurate, reliable, simple, and fast and may be used as a candidate reference method for setting target values in the standardization of serum sodium measurements." @default.
- W3029578916 created "2020-06-05" @default.
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- W3029578916 date "2020-09-01" @default.
- W3029578916 modified "2023-09-27" @default.
- W3029578916 title "Establishment and application of a new serum sodium candidate reference method" @default.
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- W3029578916 doi "https://doi.org/10.1016/j.cca.2020.05.046" @default.
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