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- W3031286095 abstract "A novel niobium nitride, U2S3-type Nb2N3, has been successfully synthesized by nitridation of δ-NbN above approximately 30 GPa in a laser-heated diamond anvil cell. Nb2N3 crystallizes in the same orthorhombic structure (space group: Pnma) as η-Ta2N3. Nb2N3 consists of regular-shaped polyhedra, and the bulk modulus has been determined to K0 = 300(2) GPa. The low-temperature X-ray diffraction measurements have been successfully conducted for the tiny novel Nb2N3 between 297.7(5) and 106.3(3) K under ambient pressure. Nb2N3 shows no structural phase transition down to 106.3(3) K, and investigation of the linear thermal expansion coefficients yields αa = 3.36(9) × 10-6 K-1, αb = 5.39(10) × 10-6 K-1, αc = 6.77(15) × 10-6 K-1, respectively. Our study reveals that the incompressible novel nitride shows low thermal expansion behavior, which offers new insights for the development of functional nitrides and their crystal chemistry." @default.
- W3031286095 created "2020-06-05" @default.
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- W3031286095 date "2020-05-28" @default.
- W3031286095 modified "2023-10-08" @default.
- W3031286095 title "Thermal Expansion of Incompressible U2S3-Type Nb2N3 Synthesized in a Diamond Anvil Cell" @default.
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- W3031286095 doi "https://doi.org/10.1021/acs.inorgchem.0c01057" @default.
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