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• W3033110681 abstract "Abstract A combination of fluorobenziodoxole (FBX) and BF 3 ⋅ OEt 2 in cyclopentyl methyl ether promotes regio‐ and stereoselective addition of benziodoxole and methoxy groups to alkynes. This difunctionalization reaction tolerates a variety of functionalized internal and terminal alkynes to afford trans ‐β‐alkoxyvinylbenziodoxoles, which represent versatile precursors to stereochemically well‐defined multisubstituted vinyl ethers. The reaction is proposed to involve cleavage of the I−F bond of FBX by BF 3 , followed by electrophilic activation of the alkyne by the resulting cationic I III species that triggers the nucleophilic addition of the ethereal oxygen." @default.
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• W3033110681 date "2020-06-24" @default.
• W3033110681 modified "2023-09-30" @default.
• W3033110681 title "Fluorobenziodoxole−BF ₃ Reagent for Iodo(III)etherification of Alkynes in Ethereal Solvent" @default.
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• W3033110681 doi "https://doi.org/10.1002/asia.202000653" @default.
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