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- W3033752761 abstract "Abstract SnO particles were synthesized by an alkali-assisted hydrothermal and microwave methods. The aqueous-based reactions were carried out at pH ~ 8, under inert atmosphere (Ar). The reactions were taken under different times, and a full XRD structural analysis was made to evaluate the conversion from the Sn 6 O 4 (OH) 4 intermediate to SnO particles. Williamson-Hall analysis showed that the size and strain of the SnO particles were time and route treatment dependent. Microwave heating yielded a single tetragonal SnO phase after 1 h of thermal treatment, and TEM images revealed spherical-shaped SnO nanoparticles with an average size of 9(1) nm. While by the hydrothermal treatment single SnO phase was obtained only after 4 hours, yielding non-uniform and elongated particles with sub-micrometric size. A dissolution-recrystallization process was taken into account as the mechanism for SnO particles formation, in which hydroxylated complexes, Sn 2 (OH) 6 −2 , then condense to form the oxide. The time-shorting reaction provided by the microwave-assisted synthesis may be attributed to better heat distribution." @default.
- W3033752761 created "2020-06-12" @default.
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- W3033752761 date "2020-06-10" @default.
- W3033752761 modified "2023-10-16" @default.
- W3033752761 title "Structural characterization of SnO nanoparticles synthesized by the hydrothermal and microwave routes" @default.
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- W3033752761 doi "https://doi.org/10.1038/s41598-020-66043-4" @default.
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