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- W3036341899 abstract "A series of binary oxides and SiC whisker reinforced composites both having a matrix composed of an α-(Al, R) 2 O 3 solid solution (R: rare earth) have been studied by analytical electron microscopy (AEM). The mechanical properties of the composites as well as crystal structure, composition, and defects of both second phases and the matrix were investigated. The formation of various second phases, e.g. garnet, β-Alumina, or perovskite structures in the binary Al 2 O 3 -R 2 O 3 and the ternary Al 2 O 3 -R 2 O 3 -SiC(w) systems are discussed. Sections of the materials having thicknesses of 100 μm - 300 μm were first diamond core drilled. The discs were then polished and dimpled. The final step was ion milling with Ar + until breakthrough occurred. Samples prepared in this manner were then analyzed using the Philips EM400T AEM. The low-Z energy dispersive X-ray spectroscopy (EDXS) data were obtained and correlated with convergent beam electron diffraction (CBED) patterns to identify phase compositions and structures. The following EDXS parameters were maintained in the analyzed areas: accelerating voltage of 120 keV, sample tilt of 12° and 20% dead time." @default.
- W3036341899 created "2020-06-25" @default.
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- W3036341899 date "1992-08-01" @default.
- W3036341899 modified "2023-09-26" @default.
- W3036341899 title "Phase identification in SiC whisker reinforced Al2O3-R2O3-based composites" @default.
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- W3036341899 doi "https://doi.org/10.1017/s0424820100121168" @default.
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