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- W3036352983 abstract "The promise of the new generation of high-voltage, high-resolution electron microscopes (HREMs) for atomic resolution studies in materials science has excited considerable interest (1). This paper describes an application to elemental Ge of the first member of this generation, the Kyoto 500kV HREM (2). Fig. 1 shows a (Oil) Ge crystal almost certainly less than 100Å thick, supported by a thin amorphous Ge film and surrounded by several Au crystallites. The specimen was prepared by vapor co-deposition of Au and Ge from separate sources onto a rock salt substrate held at room temperature. The imaging parameters were: accelerating voltage 500kV, axial illumination, no objective aperture, el. opt. mag. 200 000x, exposureotime 10 secs and, as the optical diffractogram (Fig. lb) shows, defocus =-600Å (≃ Scherzer defocus). The dashed circles in the diffractogram show the theoretical extent of the first phase-contrast transfer interval. The interval easily includes all the 111 diffraction spots, indicating that all the end-on (ill) planes and the defects they contain have been imaged faithfully and without distortion." @default.
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- W3036352983 date "1977-01-01" @default.
- W3036352983 modified "2023-09-25" @default.
- W3036352983 title "Lattice Imaging of a High-Angle Grain Boundary in Germanium at 500kv" @default.
- W3036352983 cites W36692847 @default.
- W3036352983 doi "https://doi.org/10.1017/s0424820100078158" @default.
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