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- W3036659984 abstract "A generalintermolecular anti-Michael reductiveHeck reaction of α,β-unsaturated esters with organobromideshas been developed. Most topical classes of aryl, heteroaryl, andvinyl bromides were found to efficiently react with a variety of internalconjugated alkenes. This protocol set up a platform toward diverseα-arylated 1,6-dicarbonyl frameworks found in natural productsand drugs, which are still highly challenging targets in traditionalα-arylation protocols because of competitive selectivity ofenolation. A removable directing group, gram-scale reaction, and modificationof complex molecules have additionally demonstrated that the anti-Michael reductive Heck reaction is a powerful complementarystrategy to the classical α-arylation approaches. Preliminarymechanistic studies are consistent with our proposed mechanistic design." @default.
- W3036659984 created "2020-06-25" @default.
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- W3036659984 date "2020-06-16" @default.
- W3036659984 modified "2023-09-24" @default.
- W3036659984 title "Palladium-Catalyzed <i>anti</i>-Michael Reductive Heck Reaction of α,β-Unsaturated Esters" @default.
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- W3036659984 doi "https://doi.org/10.1021/acscatal.0c02414" @default.
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