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- W3036767955 abstract "X-ray diffraction plays a dominant role in the crystal structure determinations. Typically, diffraction data of a selected single crystal is first collected by a diffractometer, and then the crystal structure can be solved and refined. The quality of the structure determination is measured by the crystallographic residual value R. If the R value is reasonably small, the structural model is assumed to be correct. Usually, models found by x-ray diffraction do describe real structures and these can be confirmed by other techniques. We report here an unusual case, a plausible structural model which yielded a low R value from data collected on a crystal that was NOT single: the structure derived from the single crystal x-ray diffraction data is completely bogus. TEM played an important role in solving this problem. In the context of high-temperature superconductivity, we have recently studied Ir +4 containing layered oxides in the SrO-IrO 2 system. Sr 2 lrO 4 has a K 2 NiF 4 -type structure with a rotational distortion (see fig. la)." @default.
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- W3036767955 date "1995-08-13" @default.
- W3036767955 modified "2023-09-25" @default.
- W3036767955 title "TEM contribution to solve the crystal structure of Sr5Ir3O11" @default.
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- W3036767955 doi "https://doi.org/10.1017/s0424820100136945" @default.
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